Publication: Sonochemical Synthesis of Nano-Scale Mixed-Ligands Lead(II) Coordination Polymers as Precursors for Preparation of PbO and PbBr(OH) Nano-Structures; Thermal, Structural and X-Ray Powder Diffraction Studies
| dc.authorscopusid | 35219300600 | |
| dc.authorscopusid | 58038557300 | |
| dc.authorscopusid | 58717985000 | |
| dc.authorscopusid | 36039473500 | |
| dc.contributor.author | Sadeghzadeh, H. | |
| dc.contributor.author | Morsali, A. | |
| dc.contributor.author | Yilmaz, V.T. | |
| dc.contributor.author | Büyuk̈güngör, O. | |
| dc.date.accessioned | 2020-06-21T14:52:38Z | |
| dc.date.available | 2020-06-21T14:52:38Z | |
| dc.date.issued | 2010 | |
| dc.department | Ondokuz Mayıs Üniversitesi | en_US |
| dc.department-temp | [Sadeghzadeh] Homa, Department of Chemistry, Tarbiat Modares University, Tehran, Tehran, Iran; [Morsali] Ali, Department of Chemistry, Tarbiat Modares University, Tehran, Tehran, Iran; [Yilmaz] Veysel T., Department of Chemistry, Bursa Uludağ Üniversitesi, Bursa, Bursa, Turkey; [Büyuk̈güngör] Orhan, Department of Physics, Ondokuz Mayis Üniversitesi, Samsun, Turkey | en_US |
| dc.description.abstract | Nano-structures of two new lead(II) two-dimensional coordination polymers, [Pb<inf>2</inf>(2-pyc)<inf>2</inf>(I)<inf>2</inf>]<inf>n</inf> (1) and [Pb<inf>2</inf>(2-pyc)<inf>2</inf>(Br)<inf>2</inf>]<inf>n</inf> (2), {2-Hpyc = 2-pyridinecarboxilic acid } were synthesized by a sonochemical method that produce the coordination polymers at nano-size. The new nano-structures were characterized by scanning electron microscopy, X-ray powder diffraction, IR spectroscopy and elemental analyses. Compounds 1 and 2 were structurally characterized by single crystal X-ray diffraction and consist of two-dimensional polymeric units. The thermal stability of compounds 1 and 2 were studied by thermal gravimetric and differential thermal analyses. PbO and PbBr(OH) nano-structures were obtained by calcination of the nano-structures of compounds 1 and 2 at 400 °C, respectively. © 2009 Elsevier B.V. All rights reserved. | en_US |
| dc.identifier.doi | 10.1016/j.ultsonch.2009.11.015 | |
| dc.identifier.endpage | 597 | en_US |
| dc.identifier.issn | 1350-4177 | |
| dc.identifier.issn | 1873-2828 | |
| dc.identifier.issue | 3 | en_US |
| dc.identifier.pmid | 20022283 | |
| dc.identifier.scopus | 2-s2.0-72649085315 | |
| dc.identifier.scopusquality | Q1 | |
| dc.identifier.startpage | 592 | en_US |
| dc.identifier.uri | https://doi.org/10.1016/j.ultsonch.2009.11.015 | |
| dc.identifier.uri | https://hdl.handle.net/20.500.12712/18056 | |
| dc.identifier.volume | 17 | en_US |
| dc.identifier.wos | WOS:000274278800016 | |
| dc.identifier.wosquality | Q1 | |
| dc.language.iso | en | en_US |
| dc.publisher | Elsevier | en_US |
| dc.relation.ispartof | Ultrasonics Sonochemistry | en_US |
| dc.relation.journal | Ultrasonics Sonochemistry | en_US |
| dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
| dc.rights | info:eu-repo/semantics/closedAccess | en_US |
| dc.subject | Coordination Polymer | en_US |
| dc.subject | Crystal Structure | en_US |
| dc.subject | Lead(II) | en_US |
| dc.subject | Nano-Structure | en_US |
| dc.title | Sonochemical Synthesis of Nano-Scale Mixed-Ligands Lead(II) Coordination Polymers as Precursors for Preparation of PbO and PbBr(OH) Nano-Structures; Thermal, Structural and X-Ray Powder Diffraction Studies | en_US |
| dc.type | Article | en_US |
| dspace.entity.type | Publication |