Browsing by Author "Harrison, WTA"
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2-(hydroxymethyl)pyridinium dihydrogenphosphate
Demir, S; Yılmaz, Veysel T.; Harrison, WTA (Int Union Crystallography, 2003)The title compound, C6H8NO+.H2PO4-, consists of 2-(hydroxymethyl)pyridinium and dihydrogenphosphate ions. The dihydrogenphosphate moieties are linked into chains by pairs of P-O-H...O-P hydrogen bonds. The 2-(hydroxymeth ... -
(3-Hydroxy-2-pyridylmethyl)dimethylammonium dihydrogen phosphate
Demir, S; Yılmaz, Veysel T.; Harrison, WTA (Int Union Crystallography, 2006)The title compound, C8H13N2O+center dot H2PO4-, is an ionic salt. The organic species is protonated at the N atom of the dimethylaminomethyl group. The dihydrogenphosphate moieties are connected into infinite chains by way ... -
Bis(2-pyridylmethanol)bis(saccharinato)zinc(II) and -cadmium(II) at 120 K: three-dimensional structures containing both N-and O-coordinated ambidentate saccharinate ligands
Yılmaz, Veysel T.; Guney, S; Andac, O; Harrison, WTA (Blackwell Munksgaard, 2002)The title complexes [M(sac)(2)(mpy)(2)] [sac is saccharinate (C7H4NO3S) and mpy is 2-pyridylmethanol (C6H7NO)], with M = Zn-II and Cd-II, are isostructural and consist of neutral molecules. The Zn-II or Cd-II cations are ... -
Bis(p-nitrobenzoxasulfamato) complexes of cadmium(II) and mercury(II) - Synthesis, spectra, and X-ray crystal structures
Yılmaz, Veysel T.; Yazicilar, TK; Andac, O; Kutuk, H; Bekdemir, Y; Harrison, WTA (Wiley-V C H Verlag Gmbh, 2002)The reaction of sodium benzoxasulfamate (ribs) with cadmium(II) and mercury(II) sulfate in aqueous solution yield the novel complexes [Cd(nbs)(2)(H2O)(4)] (1) and [Hg(nbs)(2)(H2O)(3)] (2), respectively. The complexes were ... -
Bis(pyridine-2,6-dimethanol-N,O,O ')cobalt(II) and -copper(II) disaccharinate dihydrate: three-dimensional structures with extensive hydrogen bonds and aromatic pi-pi-stacking interactions
Andac, O; Guney, S; Topcu, Y; Yılmaz, Veysel T.; Harrison, WTA (Blackwell Munksgaard, 2002)Bis(pyridine-2,6-dimethanol-N,O,O')cobalt(II) disaccharinate dihydrate, [Co(C7H9NO2)(2)](C7H4NO3S)(2).2H(2)O, (I), and bis(pyridine-2,6-dimethanol-N,O,O')copper(II) disaccharinate dihydrate, [Cu(C7H9NO2)(2)](C7H4NO3S)(2).2H(2)O, ... -
Bis(saccharinato)copper(II) complexes with 2-aminomethylpyridine and 2-aminoethylpyridine: Syntheses, crystal structures, spectral and thermal characterizations of trans-[Cu(sac)(2)(ampy)(2)] and [Cu(sac)(2)(aepy)(H2O)] (ampy=2-aminomethylpyridine and aepy=2-aminoethylpyridine)
Yılmaz, Veysel T.; Caglar, S; Harrison, WTA (Taylor & Francis Ltd, 2005)Two bis(saccharinato)copper(II) complexes with 2-aminomethylpyridine (ampy) and 2-aminoethylpyridine (aepy) have been prepared and characterized by elemental analyses, IR and electronic spectroscopy, magnetic measurements ... -
Bis(saccharinato)nickel(II) complexes with 2-aminomethyl and -ethylpyridines. Syntheses, crystal structures, spectral and thermal analyses of trans-[Ni(sac-N)(2)(ampy-N,N ')(2)] and trans-[Ni(sac-O)(2)(aepy-N,N ')(2)]
Yılmaz, Veysel T.; Caglar, S; Harrison, WTA (Kluwer Academic Publ, 2004)The trans-bis(saccharinato)nickel(II) complexes with 2-aminomethylpyridine (ampy) and 2-aminoethylpyridine (aepy) have been prepared and characterized by elemental analyses, i.r., u.v.-vis., magnetic measurements and single ... -
Bis(saccharinato-kappa N)zinc(II) complexes with N,N '-bidentate 2-aminomethylpyridine and 2-aminoethylpyridine
Yılmaz, Veysel T.; Caglar, S; Harrison, WTA (Blackwell Munksgaard, 2004)The structures of trans-bis[2-(aminomethyl) pyridine-kappa(2)N,N']bis(saccharinato-kappaN) zinc(II), [Zn(C7H4NO3S)(2)(C6H8N2)(2)], (I), and [2-(aminoethyl) pyridine-kappa2N,N'] bis(saccharinato-kappaN)zinc(II), ... -
Bis(triethanolamine-N,O,O ')nickel(II) bis(saccharinate)
Topcu, Y; Andac, O; Yılmaz, Veysel T.; Harrison, WTA (Munksgaard Int Publ Ltd, 2001)The structure of the title compound, [Ni(C6H15NO3)(2)](C7H4NO3S)(2), consists of a cationic [Ni(TEA)(2)](2+) and two anionic (SAC)(-) moieties (TEA is triethanolamine and SAC is the saccharinate anion). Two TEA ligands ... -
Bis[1-(2,6-dimethylanilino)propane-1,2-dione dioximato]nickel(II)
Bati, H; Zulfikaroglu, A; Tas, M; Andac, O; Harrison, WTA (Int Union Crystallography, 2005)The structure of the title complex consists of isolated [Ni(C11H14N3O2) (2)] units. The Ni atom is coordinated by four oxime N atoms in distorted square-planar geometry and lies on an inversion centre. The structure is ... -
A chiral coordination polymer of silver(I) with saccharinate and pyridine: Synthesis, spectral, thermal, and structural characterization of [Ag(sac)(py)](n)
Hamamci, S; Yılmaz, Veysel T.; Harrison, WTA (Springer/Plenum Publishers, 2005)The first silver(I) complex of saccharinate (sac) with pyridine (py), [Ag(sac)(py)](n) has been synthesized and characterized by elemental analysis, IR spectroscopy and single crystal X-ray diffractometry. The complex ... -
Di- and tetranuclear silver (I)-saccharinate complexes with 2-pyridineethanol and 2-pyridinepropanol: Syntheses, crystal structures, spectroscopic and thermal analyses of [Ag-2(sac)(2)(pyet)(2)] and [Ag-4(sac)(4)(pypr)(2)]
Yılmaz, Veysel T.; Hamamci, S; Harrison, WTA; Thone, C (Pergamon-Elsevier Science Ltd, 2005)Two new (saccharinato)silver (I) complexes, [Ag-2(sac)(2)(pyet)(2)] and [Ag-4(sac)(4)(pypr)(2)] (sac = saccharinate, pyet = 2-pyridineethanol and pypr = 2-pyridinepropanol), have been prepared and characterized by elemental ... -
Different coordination modes of saccharin in the metal complexes with 2-pyridylmethanol: synthesis, spectroscopic, thermal and structural characterization
Yılmaz, Veysel T.; Guney, S; Andac, O; Harrison, WTA (Pergamon-Elsevier Science Ltd, 2002)The reaction of [M(sac)(2)(H(2)O)].2H(2)O(2) where M is Mn(II), Fe(II), Co(II), Ni(II), Cu(II), Zn(II), Cd(II) and Hg(II), and sac is the saccharinate anion, with 2-pyridylmethanol (mpy) result in the formation of the new ... -
The first metal complex of p-nitrobenzoxasulfamate. Synthesis, spectral and structural characterization of triaquabis(p-nitrobenzoxasulfamato)copper(II) monohydrate
Yılmaz, Veysel T.; Andac, O; Yazicilar, TK; Kutuk, H; Bekdemir, Y; Harrison, WTA (Elsevier Science Bv, 2002)The first Cu(II) complex of p-nitrobenzoxasulfamate (nbs) was characterized by elemental analysis, IR spectroscopy and single crystal X-ray spectrometry. Triaquabis(p-nitrobenzoxasulfamate)copper(II) monohydrate, ... -
A hydrogen-bonded dimer of a novel Co(II) complex of monoethanolamine with thiocyanate: synthesis, spectra, thermal behaviour and crystal structure
Yılmaz, Veysel T.; Andac, O; Karadag, A; Harrison, WTA (Elsevier Science Bv, 2002)A strongly hydrogen-bonded dimer of the Co(II) complex of monoethanolamine, [Co(meaH)(3)][Co(mea)(meaH)(2)](SCN)(3), was synthesized and characterized by single crystal X-ray diffractometry, UV-Vis and IR spectroscopy. The ... -
Mixed-ligand metal succinate complexes with 1,10-phenanthroline and ethylenediamine: Synthesis, characterization, spectroscopic and thermal studies. Crystal structure of succinatocobalt(II) complex with phenanthroline
Yılmaz, Veysel T.; Demir, S; Andac, O; Harrison, WTA (Taylor & Francis Ltd, 2002)The novel mixed-ligand metal succinate (suc) complexes with 1, 10-phenanthroline (phen) and ethylenediamine (en) have been synthesized and characterized by elemental analyses, magnetic moments, UV-VIS and IR spectra. Thermal ... -
Mono- and binuclear copper(II) complexes of saccharin with 2-pyridinepropanol synthesis, spectral, thermal and structural characterization
Yılmaz, Veysel T.; Hamamci, S; Andac, O; Thone, C; Harrison, WTA (Springer, 2003)Mono- and binuclear copper(II) saccharinate (sac) complexes containing 2-pyridinepropanol (pypr) have been prepared and characterized by elemental analyses, i.r., u.v.-vis., magnetic measurements and single crystal X-ray ... -
N-(2-Hydroxyethyl)ethylene-diammonium hydrogenphosphate monohydrate
Demir, S; Yılmaz, Veysel T.; Andac, O; Harrison, WTA (Blackwell Munksgaard, 2002)The title compound, C4H14N2O2+.HPO42-.H2O, contains alternating interleaved layers of hydrogenphosphate and N(2-hydroxyethyl)ethylenediammonium moieties. The water molecules are associated with channel-like voids in the ... -
A new one-dimensional coordination polymer of silver(I) with bridging 2-(2-aminoethyl)pyridine and nitrato ligands: [Ag-2(mu-NO3)(2)(mu-aepy)(2)](n)
Senel, E; Yılmaz, Veysel T.; Harrison, WTA (Walter De Gruyter Gmbh, 2005)A new silver(I) nitrate complex of 2-(2-aminoethyl)pyridine (aepy), [Ag-2(mu-NO3)(2)(mu-aepy)(2)](n), has been synthesized and characterized by elemental analysis, IR spectroscopy and single crystal X-ray diffractometry. ... -
A one-dimensional lead(II) coordination polymer with bridging saccharinate and 2-aminomethylpyridine ligands: Synthesis, IR spectra, and crystal structure of [Pb(ampy)(mu-sac)(2)](n)
Yılmaz, Veysel T.; Caglar, S; Harrison, WTA (Wiley-V C H Verlag Gmbh, 2004)A complex with eight-coordinate lead(n) atom and saccharinate (sac) and 2-aminomethylpyridine ligands was characterized by IR, elemental analysis and X-ray crystallography. The lead(II) complex crystallizes in the monoclinic ...