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A new one-dimensional coordination polymer of silver(I) with bridging 2-(2-aminoethyl)pyridine and nitrato ligands: [Ag-2(mu-NO3)(2)(mu-aepy)(2)](n)

Date

2005

Author

Senel, E
Yılmaz, Veysel T.
Harrison, WTA

Metadata

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Abstract

A new silver(I) nitrate complex of 2-(2-aminoethyl)pyridine (aepy), [Ag-2(mu-NO3)(2)(mu-aepy)(2)](n), has been synthesized and characterized by elemental analysis, IR spectroscopy and single crystal X-ray diffractometry. Two silver(l) ions are doubly bridged by two bidentate aepy ligands forming dimeric building block [Ag-2(mu-aepy)(2)] units with a Ag (...) Ag distance of 3.0587(17) angstrom. These dimeric units are further doubly bridged by two nitrato ligands into a one-dimensional polymeric chain. The nitrato ligand exhibits an uncommon bidentate bridging mode of Ag-ONO-Ag. The title complex features a hydrogen bonded two-dimensional supramolecular framework formed via N-H (...) O hydrogen bonds, involving the uncoordinated O atom of the nitrate ligand and amine hydrogen atoms of aepy. The thermal stability of the title complex was investigated using thermogravimetry and differential thermal analysis.

Source

Zeitschrift Fur Naturforschung Section B-A Journal of Chemical Sciences

Volume

60

Issue

6

URI

https://hdl.handle.net/20.500.12712/21095

Collections

  • Scopus İndeksli Yayınlar Koleksiyonu [14046]
  • WoS İndeksli Yayınlar Koleksiyonu [12971]



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