Publication:
Spectroscopic Studies and Crystal Structure of 4-(2 3-Methoxybenzylideneamino) Benzenesulfonamide

dc.authorscopusid35567635300
dc.authorscopusid55905669900
dc.authorscopusid8905690500
dc.authorscopusid8220216800
dc.contributor.authorYildiz, M.
dc.contributor.authorÜnver, H.
dc.contributor.authorErdener, D.
dc.contributor.authorÍskeleli, N.O.
dc.date.accessioned2020-06-21T14:47:30Z
dc.date.available2020-06-21T14:47:30Z
dc.date.issued2010
dc.departmentOndokuz Mayıs Üniversitesien_US
dc.department-temp[Yildiz] Mustafa, Department of Chemistry, C ̧ anakkale Onsekiz Mart University, Canakkale, 17100 Çanakkale, Turkey; [Ünver] Hüseyin, Department of Physics, Ankara Üniversitesi, Ankara, Turkey; [Erdener] Diǧdem, Department of Chemistry, C ̧ anakkale Onsekiz Mart University, Canakkale, 17100 Çanakkale, Turkey; [Ískeleli] Nazan Ocak, Department of Physics, Ondokuz Mayis Üniversitesi, Samsun, Turkeyen_US
dc.description.abstractSchiff base 4-[(2-hydroxy-3-methoxybenzylideneamino)- N-(5-methylisoxazol- 3-yl)benzene-sulfonamide has been synthesized from the reaction of 4-amino-N-(5-methylisoxazol- 3-yl)benzenesulfonamide(sulfamethoxazole) with 2-hydroxy-3-methoxybenzaldehyde. It has been characterized by elemental analysis, MS, IR, 1H NMR, 13C NMR, HETCOR and UV-Visible techniques. The structure of it also has been examined crystallographically. For the compound exist as dominant form of enol-imines in both the solid state and the solutions. It crystallizes in the monoclinic space group P2<inf>1</inf>/c with a = 8.2694(7), b = 8.3453(5), c = 26.260(2) A ̊ , b = 97.142(7)°, V = 1798.1(2) A ̊ 3, D<inf>x</inf> = 1.431 g cm-3, R<inf>1</inf> = 0.0529 and wR<inf>2</inf> = 0.1370 [I[2σ(I)], respectively. © Springer Science+Business Media, LLC 2010.en_US
dc.identifier.doi10.1007/s10870-010-9723-9
dc.identifier.endpage695en_US
dc.identifier.issn1074-1542
dc.identifier.issn1572-8854
dc.identifier.issue8en_US
dc.identifier.scopus2-s2.0-77956765814
dc.identifier.scopusqualityQ4
dc.identifier.startpage691en_US
dc.identifier.urihttps://doi.org/10.1007/s10870-010-9723-9
dc.identifier.volume40en_US
dc.identifier.wosWOS:000279197600012
dc.identifier.wosqualityQ4
dc.language.isoenen_US
dc.publisherSpringer/Plenum Publishersen_US
dc.relation.ispartofJournal of Chemical Crystallographyen_US
dc.relation.journalJournal of Chemical Crystallographyen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCrystal Structureen_US
dc.subjectHydrogen Bondsen_US
dc.subjectSchiff Baseen_US
dc.subjectSpectroscopyen_US
dc.subjectTautomerismen_US
dc.titleSpectroscopic Studies and Crystal Structure of 4-(2 3-Methoxybenzylideneamino) Benzenesulfonamideen_US
dc.typeArticleen_US
dspace.entity.typePublication

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