Publication:
Crystal Structure, Spectral and Thermal Properties of Potassium p-Nitrobenzoxasulfamate Monohydrate

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dc.authorscopusid7801686683
dc.authorscopusid6701793097
dc.authorscopusid8059657200
dc.authorscopusid58717985000
dc.authorscopusid6602932193
dc.contributor.authorBekdemir, Y.
dc.contributor.authorKütük, H.
dc.contributor.authorCelik, S.
dc.contributor.authorYilmaz, V.T.
dc.contributor.authorThoene, C.
dc.date.accessioned2020-06-21T15:48:53Z
dc.date.available2020-06-21T15:48:53Z
dc.date.issued2002
dc.departmentOndokuz Mayıs Üniversitesien_US
dc.department-temp[Bekdemir] Yunus, Department of Chemistry, Ondokuz Mayis Üniversitesi, Samsun, Turkey; [Kütük] Halil, Department of Chemistry, Ondokuz Mayis Üniversitesi, Samsun, Turkey; [Celik] Sibel, Department of Chemistry, Ondokuz Mayis Üniversitesi, Samsun, Turkey; [Yilmaz] Veysel T., Department of Chemistry, Ondokuz Mayis Üniversitesi, Samsun, Turkey; [Thoene] Carsten, Institut für Anorganische und Analytische Chemie, Technische Universität Braunschweig, Braunschweig, Niedersachsen, Germanyen_US
dc.description.abstractThe potassium p-nitrobenzoxasulfamate monohydrate salt (C<inf>6</inf>H<inf>3</inf>N<inf>2</inf>O<inf>5</inf> SK·H<inf>2</inf>O), was prepared by the reaction of p-nitrobenzoxasulfamate with t-BuOK in the water-THF solution and characterized by C, H, N, S analyses, IR, UV-VIS and 1H NMR spectroscopy. The structure of the compound has been determined by single-crystal X-ray diffraction. The compound crystallizes in orthorhombic system, space group P2<inf>1</inf>2<inf>1</inf>2<inf>1</inf>, with Z = 8. The structure consists of chains formed by K polyhedra connected by sulfonyl, nitro and amine groups of the p-nitrobenzoxasulfamate anion and lattice water molecules. Thermal decomposition behavior of the compound was studied by DTA and TG techniques. © 2002 Elsevier Science B.V. All rights reserved.en_US
dc.identifier.doi10.1016/S0022-2860(01)00659-7
dc.identifier.endpage244en_US
dc.identifier.issn0022-2860
dc.identifier.scopus2-s2.0-0037028529
dc.identifier.scopusqualityQ1
dc.identifier.startpage239en_US
dc.identifier.urihttps://doi.org/10.1016/S0022-2860(01)00659-7
dc.identifier.volume604en_US
dc.identifier.wosWOS:000173859500014
dc.identifier.wosqualityQ2
dc.language.isoenen_US
dc.publisherElsevier Science BVen_US
dc.relation.ispartofJournal of Molecular Structureen_US
dc.relation.journalJournal of Molecular Structureen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subject3H-6-Nitro-1,2,3en_US
dc.subjectBenzoxasulfamateen_US
dc.subjectBenzoxathiazole 2,2-Dioxideen_US
dc.subjectCrystal Structureen_US
dc.subjectCyclic Sulfamateen_US
dc.subjectSpectraen_US
dc.subjectThermal Analysisen_US
dc.titleCrystal Structure, Spectral and Thermal Properties of Potassium p-Nitrobenzoxasulfamate Monohydrateen_US
dc.typeArticleen_US
dspace.entity.typePublication

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