Publication: Crystal and Molecular Structure of 11,12-Dibromo-7,8-Benzo-1,5-di(p-Tolylsulphonyl)-1,5-Diazacyclononan
| dc.contributor.author | Öztürk S. | |
| dc.contributor.author | Isik S. | |
| dc.contributor.author | Fun H.-K. | |
| dc.contributor.author | Agar E. | |
| dc.contributor.author | Sasmaz S. | |
| dc.contributor.author | Büyükgüngör, Orhan | |
| dc.date.accessioned | 2020-06-21T09:15:22Z | |
| dc.date.available | 2020-06-21T09:15:22Z | |
| dc.date.issued | 2000 | |
| dc.department | OMÜ | en_US |
| dc.department-temp | Öztürk, S., Dept. of Physics, Faculty of Arts and Sciences, Erciyes University, Kayseri, Turkey -- Isik, S., Dept. of Physics, Faculty of Arts and Sciences, Ondokuz Mayis University, Samsun, Turkey, Ondokuz Mayis University, Faculty of Art and Science, Dept. Physics, 55139-Kurupelit, Samsun, Turkey -- Fun, H.-K., X-ray Crystallography Unit, School of Physics, Universiti Sains Malaysia, Penang, Malaysia -- Agar, E., Dept. of Chemistry, Faculty of Arts and Sciences, Ondokuz Mayis University, Samsun, Turkey -- Sasmaz, S., Dept. of Chemistry, Faculty of Arts and Sciences, Ondokuz Mayis University, Samsun, Turkey -- Büyükgüngör, O., Dept. of Physics, Faculty of Arts and Sciences, Ondokuz Mayis University, Samsun, Turkey -- | en_US |
| dc.description.abstract | The crystal structure of the title compound, C25H26Br2N2O4S2 was determined by single crystal X-ray diffraction technique. The crystals are monoclinic, space group C 2/c, with a = 20.7142(2) angstroms b = 11.7910(2) angstroms, c = 10.6735(3) angstroms, ? = 98.549(2)°, V = 2577.94(9) angstroms3, Z = 4. The structure was solved by direct methods and refined by least-squares methods to a final R = 0.046 for 1866 observed reflections with I>2?(I). The title compound, displays disordered geometry around the Cl atom located almost on twofold axis. The nine-membered heterocylic ring is close to the half-chair conformation. The dihedral angle between phenyl rings is 34.2(1)°. | en_US |
| dc.identifier.doi | 10.1002/1521-4079(200009)35:9<1125 | |
| dc.identifier.endpage | 1130 | en_US |
| dc.identifier.issn | 0232-1300 | |
| dc.identifier.issue | 9 | en_US |
| dc.identifier.startpage | 1125 | en_US |
| dc.identifier.uri | https://doi.org/10.1002/1521-4079(200009)35:9<1125 | |
| dc.identifier.uri | https://hdl.handle.net/20.500.12712/2702 | |
| dc.identifier.volume | 35 | en_US |
| dc.language.iso | en | en_US |
| dc.publisher | Akademie Verlag GmbH, Weinheim, Germany | en_US |
| dc.relation.journal | Crystal Research and Technology | en_US |
| dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
| dc.rights | info:eu-repo/semantics/closedAccess | en_US |
| dc.title | Crystal and Molecular Structure of 11,12-Dibromo-7,8-Benzo-1,5-di(p-Tolylsulphonyl)-1,5-Diazacyclononan | en_US |
| dc.type | Article | en_US |
| dspace.entity.type | Publication |