Publication:
Hydrothermal and Sonochemical Synthesis of a Nano-Sized 2D Lead(II) Coordination Polymer: A Precursor for Nano-Structured PbO and PbBr2

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dc.authorscopusid35809865200
dc.authorscopusid58038557300
dc.authorscopusid58717985000
dc.authorscopusid8600292400
dc.contributor.authorAslani, A.
dc.contributor.authorMorsali, A.
dc.contributor.authorYilmaz, V.T.
dc.contributor.authorKazak, C.
dc.date.accessioned2020-06-21T15:06:16Z
dc.date.available2020-06-21T15:06:16Z
dc.date.issued2009
dc.departmentOndokuz Mayıs Üniversitesien_US
dc.department-temp[Aslani] Alireza, Department of Chemistry, Tarbiat Modares University, Tehran, Tehran, Iran; [Morsali] Ali, Department of Chemistry, Tarbiat Modares University, Tehran, Tehran, Iran; [Yilmaz] Veysel T., Department of Chemistry, Bursa Uludağ Üniversitesi, Bursa, Bursa, Turkey; [Kazak] Canan, Department of Physics, Ondokuz Mayis Üniversitesi, Samsun, Turkeyen_US
dc.description.abstractA new nano-structured lead(II) coordination polymer, [Pb(μ-bpp)(μ-Br)<inf>2</inf>]<inf>n</inf> (PBB) [bpp = 1,3-di(4-pyridyl)propane], has been synthesized by the reaction of a mixture lead(II) acetate and KBr with bpp by both hydrothermal and sonochemical methods. Reaction conditions, such as temperature, time, concentration and initial reagents play important roles in the size, morphology and crystal growth of the final products. The nano-sized PbBr<inf>2</inf> and PbO were prepared from the calcination of the nano-structured PBB at vacuum and air atmosphere. The structure of PBB was determined by X-ray crystallography, while nano-structural materials were characterized by X-ray powder diffraction (XRPD) and scanning electron microscopy (SEM). Thermal stability of bulk and nano-sized particles of PBB was studied and compared with each other. © 2009 Elsevier B.V. All rights reserved.en_US
dc.identifier.doi10.1016/j.molstruc.2009.04.026
dc.identifier.endpage192en_US
dc.identifier.issn0022-2860
dc.identifier.scopus2-s2.0-67349229132
dc.identifier.scopusqualityQ1
dc.identifier.startpage187en_US
dc.identifier.urihttps://doi.org/10.1016/j.molstruc.2009.04.026
dc.identifier.urihttps://hdl.handle.net/20.500.12712/18540
dc.identifier.volume929en_US
dc.identifier.wosWOS:000267502600027
dc.identifier.wosqualityQ2
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofJournal of Molecular Structureen_US
dc.relation.journalJournal of Molecular Structureen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCoordination Polymeren_US
dc.subjectLead(II) Bromideen_US
dc.subjectLead(II) Oxideen_US
dc.subjectNano-Structureen_US
dc.titleHydrothermal and Sonochemical Synthesis of a Nano-Sized 2D Lead(II) Coordination Polymer: A Precursor for Nano-Structured PbO and PbBr2en_US
dc.typeArticleen_US
dspace.entity.typePublication

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