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Spectroscopic, Thermal and Crystal Structure Properties of Novel (E)-2,6 Acrylate Dye

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dc.authorscopusid6602199609
dc.authorscopusid55797807700
dc.authorscopusid8385454700
dc.authorscopusid7004176074
dc.contributor.authorKocaokutgen, H.
dc.contributor.authorGür, M.
dc.contributor.authorSoylu, M.S.
dc.contributor.authorLönnecke, P.
dc.date.accessioned2020-06-21T15:30:09Z
dc.date.available2020-06-21T15:30:09Z
dc.date.issued2005
dc.departmentOndokuz Mayıs Üniversitesien_US
dc.department-temp[Kocaokutgen] Hasan, Department of Chemistry, Ondokuz Mayis Üniversitesi, Samsun, Turkey; [Gür] Mahmut, Department of Chemistry, Ondokuz Mayis Üniversitesi, Samsun, Turkey; [Soylu] Mustafa Serkan, Department of Physics, Ondokuz Mayis Üniversitesi, Samsun, Turkey; [Lönnecke] Peter, Fak. für Chemie und Mineralogie, Universität Leipzig, Leipzig, Sachsen, Germanyen_US
dc.description.abstract2,6-Dimethyl-4-(4-tert-butylphenyldiazenyl)phenyl acrylate (C<inf>21</inf>H<inf>24</inf>N<inf>2</inf>O<inf>2</inf>), containing an acryloyloxy group, first 2,6-dimethyl-4-(4-tert-butylphenyldiazenyl) phenol was prepared by reacting 4-tert-butylbenzenediazonium salt with 2,6-dimethylphenol and then its acryloyloxy derivative was synthesized in a Schotten-Bauman-type reaction. The characterisation of the synthesized azo-ester dye has been described by IR, UV-vis, 1H NMR, 13C NMR spectroscopic techniques, and elemental analysis. The structure of the present compound has been determined by single-crystal X-ray diffraction. This synthesized azo-ester compound crystallizes in monoclinic system, space group P21/c with Z = 4. The thermal behaviour of the compound has been determined by means of differential thermal analysis (DTA) and thermogravimetry (TG) techniques. © 2004 Elsevier Ltd. All rights reserved.en_US
dc.identifier.doi10.1016/j.dyepig.2004.09.021
dc.identifier.endpage103en_US
dc.identifier.issn0143-7208
dc.identifier.issn1873-3743
dc.identifier.issue2en_US
dc.identifier.scopus2-s2.0-14644444570
dc.identifier.scopusqualityQ2
dc.identifier.startpage99en_US
dc.identifier.urihttps://doi.org/10.1016/j.dyepig.2004.09.021
dc.identifier.volume67en_US
dc.identifier.wosWOS:000227937000003
dc.identifier.wosqualityQ1
dc.language.isoenen_US
dc.publisherElsevier Sci Ltden_US
dc.relation.ispartofDyes and Pigmentsen_US
dc.relation.journalDyes and Pigmentsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectAcrylateen_US
dc.subjectAzo-Ester Dyesen_US
dc.subjectCrystal Structureen_US
dc.subjectDiazenesen_US
dc.subjectSpectral and Thermal Analysisen_US
dc.titleSpectroscopic, Thermal and Crystal Structure Properties of Novel (E)-2,6 Acrylate Dyeen_US
dc.typeArticleen_US
dspace.entity.typePublication

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