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Spectroscopic and Polarographic Studies of Novel Imidazole Adduct of Ammonium Trioxovanadate(V). A Solution and Solid State Study

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dc.authorscopusid55774433600
dc.authorscopusid6603524165
dc.authorscopusid7006839507
dc.authorscopusid7004387719
dc.contributor.authorÇakir, S.
dc.contributor.authorBiçer, E.
dc.contributor.authorNaumov, P.
dc.contributor.authorÇakir, O.
dc.date.accessioned2020-06-21T15:49:23Z
dc.date.available2020-06-21T15:49:23Z
dc.date.issued2001
dc.departmentOndokuz Mayıs Üniversitesien_US
dc.department-temp[Çakir] Semiha, Department of Chemistry, Ondokuz Mayis Üniversitesi, Samsun, Turkey; [Bi̇Çer] Ender, Department of Chemistry, Ondokuz Mayis Üniversitesi, Samsun, Turkey; [Naumov] PanČe, Institute of Chemistry, Ss. Cyril and Methodius University in Skopje, Skopje, North Macedonia; [Çakir] Osman, Department of Chemistry, Ondokuz Mayis Üniversitesi, Samsun, Turkeyen_US
dc.description.abstractComplex formation between ammonium trioxovanadate(V) and imidazole has been studied and characterized by FT IR, UV/Vis, thermal analysis (TG, DTA, DTG) and polarographic techniques. Species formed in solid phase yield a yellow coloured product exhibiting an absorbance maximum at 400 nm. The FT IR spectra show that the inclusion of imidazole has a significant influence on the structure and the hydrogen bonding pattern in NH<inf>4</inf>VO<inf>3</inf>. Species formed in aqueous solution has been examined by voltammetry. Formation of an adduct of trioxovanadate(V) with imidazole onto dropping mercury electrode followed by reduction of the sample in DCP of the complex in 0.05 M NH<inf>3</inf>/NH<inf>4</inf>Cl buffer (pH 9.08) resulted in a single peak at -0.875 V.en_US
dc.identifier.endpage214en_US
dc.identifier.issn0137-5083
dc.identifier.issue2en_US
dc.identifier.scopus2-s2.0-0035530970
dc.identifier.startpage209en_US
dc.identifier.volume75en_US
dc.identifier.wosWOS:000167001700002
dc.language.isoenen_US
dc.publisherPolish Chemical Societyen_US
dc.relation.ispartofPolish Journal of Chemistryen_US
dc.relation.journalPolish Journal of Chemistryen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectAmmonium Trioxovanadate(V)en_US
dc.subjectFt Iren_US
dc.subjectImidazole Adducten_US
dc.subjectThermal Analysisen_US
dc.subjectUv/Visen_US
dc.subjectVoltammetryen_US
dc.titleSpectroscopic and Polarographic Studies of Novel Imidazole Adduct of Ammonium Trioxovanadate(V). A Solution and Solid State Studyen_US
dc.typeArticleen_US
dspace.entity.typePublication

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