Synthesis, Spectral Properties and Structure of New Novel 3,3'-Dibenzoyl-1,1'-(Propan-1,3-diyl)-Bisthiourea

Abstract

A new 3,3'-dibenzoyl-1,1'-propan-1,3-diyl)bisthiourea was synthesized by using benzoylisothiocyanate with 1,3-diaminopropane in aprotic solvent. The structure was determinated by means of FT-IR, 1H-NMR, 13C-NMR and mass spectroscopic techniques. The crystal structure of 3,3'-dibenzoyl-1,1'-(propan-1,3-diyl)bisthiourea has also been examined by using X-ray crystallographic techniques and found to be crystallized in the monoclinic space group P2 <inf>1</inf>/c with the unit cell parameters: a = 5.968(1) Å, b = 19.471(2) Å, c = 16.585(2) Å, β = 98.32(1)°, V = 1907.0 (4) Å 3, Dx = 1.395 g cm -3, and Z = 4 respectively. © Springer Science+Business Media, LLC 2012.