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Synthesis, Crystal Structure, Spectroscopic and Thermal Characterization of (Hampy)2[Ni(pydc)2(H2O)2] · 2 H2O

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dc.authorscopusid16021063600
dc.authorscopusid26632875300
dc.authorscopusid16403949600
dc.authorscopusid36039473500
dc.contributor.authorÇolak, A.T.
dc.contributor.authorAkduman, D.
dc.contributor.authorYeşilel, O.Z.
dc.contributor.authorBüyuk̈güngör, O.
dc.date.accessioned2020-06-21T15:12:42Z
dc.date.available2020-06-21T15:12:42Z
dc.date.issued2009
dc.departmentOndokuz Mayıs Üniversitesien_US
dc.department-temp[Çolak] Alper Tolga, Department of Chemistry, Dumlupinar Üniversitesi, Kutahya, Turkey; [Akduman] Demet, Department of Chemistry, Dumlupinar Üniversitesi, Kutahya, Turkey; [Yeşilel] Okan Zafer, Department of Chemistry, Eskişehir Osmangazi Üniversitesi, Eskisehir, Eskisehir, Turkey; [Büyuk̈güngör] Orhan, Department of Physics, Ondokuz Mayis Üniversitesi, Samsun, Turkeyen_US
dc.description.abstractA supramolecular complex, bis(2-amino-3-rnethylpyridinium) diaquabis(pyridinedicarboxylato)nickelate(II) dihydrate, (Hampy) <inf>2</inf>[Ni(pydc)<inf>2</inf>(H<inf>2</inf>O)<inf>2</inf>] • 2 H <inf>2</inf>O (ampy = 2-amino-3-methylpyridine, H<inf>2</inf>pydc = 2,5-pyridinedicarboxylic acid or isocinchomeronic acid) (1) has been prepared and characterized by elemental, spectral (IR and UV-vis.), thermal analysis, magnetic measurement and single crystal X-ray diffraction techniques. Ni(II) ion exhibits a distorted octahedral geometry coordinated by nitrogen and oxygen atoms of two pyridinedi-carboxylate ligands, oxygen atoms from the two aqua ligands. The supramolecular network is constructed by N-H • • • O strong hydrogen bonds, π - π and C-H • . • π interactions. © by Oldenbourg Wissenschaftsverlag, München.en_US
dc.identifier.doi10.1524/zkri.2009.1112
dc.identifier.endpage212en_US
dc.identifier.issn0044-2968
dc.identifier.issue4en_US
dc.identifier.scopus2-s2.0-65949100146
dc.identifier.startpage207en_US
dc.identifier.urihttps://doi.org/10.1524/zkri.2009.1112
dc.identifier.volume224en_US
dc.identifier.wosWOS:000265807900003
dc.language.isoenen_US
dc.publisherOldenbourg Verlagen_US
dc.relation.ispartofZeitschfrift für Kristallographieen_US
dc.relation.journalZeitschrift Fur Kristallographieen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subject2,5-Pyridinedicarboxylicen_US
dc.subject2-Amino-3-Methylpyridineen_US
dc.subjectNickel(II)en_US
dc.subjectSingle Crystal Structure Analysisen_US
dc.subjectX-Ray Diffractionen_US
dc.titleSynthesis, Crystal Structure, Spectroscopic and Thermal Characterization of (Hampy)2[Ni(pydc)2(H2O)2] · 2 H2Oen_US
dc.typeArticleen_US
dspace.entity.typePublication

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