Publication:
The Clean and Mild Synthesis, Crystal Structure, and Intra-Molecular Hydrogen Bond Study of Substituted New 4,8-Dihydropyrano[3,2-B]-Pyrans Containing Chlorokojic Acid Moiety

dc.authorscopusid57205386708
dc.authorscopusid26668005400
dc.authorscopusid8954286200
dc.authorscopusid57201620841
dc.authorscopusid55550270900
dc.contributor.authorOjaghi Aghbash, K.
dc.contributor.authorNoroozi-Pesyan, N.
dc.contributor.authorMarandi, G.
dc.contributor.authorDege, N.
dc.contributor.authorŞahin, E.
dc.date.accessioned2020-06-21T12:26:06Z
dc.date.available2020-06-21T12:26:06Z
dc.date.issued2019
dc.departmentOndokuz Mayıs Üniversitesien_US
dc.department-temp[Ojaghi Aghbash] Khadijeh, Department of Organic Chemistry, Urmia University, Urmia, Iran; [Noroozi-Pesyan] Nader, Department of Organic Chemistry, Urmia University, Urmia, Iran; [Marandi] G., Department of Organic Chemistry, Urmia University, Urmia, Iran; [Dege] Necmi, Department of Physics, Ondokuz Mayis Üniversitesi, Samsun, Turkey; [Şahin] Ertan, Department of Chemistry, Atatürk Üniversitesi, Erzurum, Erzurum, Turkeyen_US
dc.description.abstractA safe, green and convenient process was developed for the synthesis of a novel group of 4,8-dihydropyrano[3,2-b]-pyrans by dialkyl acetylenedicarboxylates and alkyl isocyanides being trapped by chlorokojic acid in good to excellent yields at ambient temperature. Characterization of all structures was carried out by FT-IR and 1H and 13C NMR spectrometers, and two compounds were analyzed using X-ray diffraction technique. Crystal structures showed an intramolecular hydrogen bond and stacking of the dimeric (RS) molecules with the unit cell along the a-axis. © 2019, Springer Nature B.V.en_US
dc.identifier.doi10.1007/s11164-019-03848-7
dc.identifier.endpage4554en_US
dc.identifier.issn0922-6168
dc.identifier.issn1568-5675
dc.identifier.issue9en_US
dc.identifier.scopus2-s2.0-85065736754
dc.identifier.scopusqualityQ2
dc.identifier.startpage4543en_US
dc.identifier.urihttps://doi.org/10.1007/s11164-019-03848-7
dc.identifier.volume45en_US
dc.identifier.wosWOS:000481805000020
dc.identifier.wosqualityQ2
dc.language.isoenen_US
dc.publisherSpringer Science and Business Media B.V.en_US
dc.relation.ispartofResearch on Chemical Intermediatesen_US
dc.relation.journalResearch on Chemical Intermediatesen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subject4,8-Dihydropyrano[3,2-b]-Pyranen_US
dc.subject4H-Pyranen_US
dc.subjectAcetylene Estersen_US
dc.subjectChlorokojic Aciden_US
dc.subjectIntramolecular H Bonden_US
dc.subjectInversion Dimersen_US
dc.subjectIsocyanidesen_US
dc.subjectNucleophilic Additionen_US
dc.titleThe Clean and Mild Synthesis, Crystal Structure, and Intra-Molecular Hydrogen Bond Study of Substituted New 4,8-Dihydropyrano[3,2-B]-Pyrans Containing Chlorokojic Acid Moietyen_US
dc.typeArticleen_US
dspace.entity.typePublication

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