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dc.contributor.authorAkkurt M.
dc.contributor.authorYildirim S.O.
dc.contributor.authorŞreci N.
dc.contributor.authorKüçükbay H.
dc.contributor.authorBüyükgüngör, Orhan
dc.date.accessioned2020-06-21T09:27:22Z
dc.date.available2020-06-21T09:27:22Z
dc.date.issued2007
dc.identifier.issn1348-2238
dc.identifier.urihttps://doi.org/10.2116/analscix.23.x233
dc.identifier.urihttps://hdl.handle.net/20.500.12712/4027
dc.description.abstractThe title compound, (2E)-3-(2-thienyl)acrylic acid-benzene-1,2-diamine, was synthesized by the reaction of 1,2-diaminobenzen and 3-(2-tienyl)acrylic acide in a dioxane solution. The compound crystallizes in the orthorhombic space group Pbcn; a = 24.610(5)Å, b = 7.588(5)Å, c = 11.289(5)Å, V = 2108.1(17)Å3 and Z = 8. The final R value is 0.047. The thiophene and benzene ring are each essentially planar. The benzene-1,2-diamine moity in the title compound has a rotation axis that passes through the mid point of the bonds C8-C8a and C10-C10a. The crystal packing is stabilized by intermolecular N-H···and O-H···N hydrogen-bonding interactions. 2007 © The Japan Society for Analytical Chemistry.en_US
dc.language.isoengen_US
dc.publisherJapan Society for Analytical Chemistryen_US
dc.relation.isversionof10.2116/analscix.23.x233en_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.titleCrystal structure of (2E)-3-(2-thienyl)acrylic acid-benzene-1,2-diamineen_US
dc.typenoteen_US
dc.contributor.departmentOMÜen_US
dc.identifier.volume23en_US
dc.identifier.issue11en_US
dc.identifier.startpagex233en_US
dc.identifier.endpagex234en_US
dc.relation.journalAnalytical Sciences: X-ray Structure Analysis Onlineen_US
dc.relation.publicationcategoryDiğeren_US


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