dc.contributor.author | Daoui S. | |
dc.contributor.author | Baydere C. | |
dc.contributor.author | Kalai F.E. | |
dc.contributor.author | Saddik R. | |
dc.contributor.author | Dege N. | |
dc.contributor.author | Karrouchi K. | |
dc.contributor.author | Benchat N. | |
dc.date.accessioned | 2020-06-21T09:05:20Z | |
dc.date.available | 2020-06-21T09:05:20Z | |
dc.date.issued | 2019 | |
dc.identifier.issn | 2056-9890 | |
dc.identifier.uri | https://doi.org/10.1107/S2056989019014130 | |
dc.identifier.uri | https://hdl.handle.net/20.500.12712/2295 | |
dc.description.abstract | In the title compound, C13H14N2O3, the dihydropyridazine ring (r.m.s. deviation = 0.166 Å) has a screw-boat conformation. The dihedral angle between its mean plane and the benzene ring is 0.77 (12)°. In the crystal, intermolecular O-H..O hydrogen bonds generate C(5) chains and N-H..O hydrogen bonds produce R 2 2(8) motifs. These types of interactions lead to the formation of layers parallel to (12). The three-dimensional network is achieved by C-H..O interactions, including R 2 4(8) motifs. Intermolecular interactions were additionally investigated using Hirshfeld surface analysis and two-dimensional fingerprint plots. The most significant contributions to the crystal packing are by H..H (43.3%), H..C/C..H (19.3%), H..O/H..O (22.6%), C..N/N..C (3.0%) and H..N/N..H (5.8%) contacts. C-H..? interactions and aromatic ?-? stacking interactions are not observed. © 2019 International Union of Crystallography. All rights reserved. | en_US |
dc.description.sponsorship | Fundamental Research Fund of Shandong University Faculty of Arts and Sciences, Harvard University | en_US |
dc.description.sponsorship | The authors acknowledge the Faculty of Arts and Sciences, Ondokuz Mayıs University, Turkey, for the use of the Stoe IPDS 2 diffractometer (purchased under grant F.279 of the University Research Fund). | en_US |
dc.language.iso | eng | en_US |
dc.publisher | International Union of Crystallography | en_US |
dc.relation.isversionof | 10.1107/S2056989019014130 | en_US |
dc.rights | info:eu-repo/semantics/openAccess | en_US |
dc.subject | Crystal structure | en_US |
dc.subject | Hirshfeld surface analysis | en_US |
dc.subject | Hydrogen bonding | en_US |
dc.subject | Pyridazine | en_US |
dc.title | Crystal structure and Hirshfeld surface analysis of (E)-6-(4-hydroxy-3-methoxystyryl)-4,5-dihydropyridazin-3(2H)-one | en_US |
dc.type | article | en_US |
dc.contributor.department | OMÜ | en_US |
dc.identifier.volume | 75 | en_US |
dc.identifier.startpage | 1734 | en_US |
dc.identifier.endpage | 1737 | en_US |
dc.relation.journal | Acta Crystallographica Section E: Crystallographic Communications | en_US |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |