dc.contributor.author | Odabaşoğlu, Mustafa | |
dc.contributor.author | Büyükgüngör, Orhan | |
dc.contributor.author | Turgut, G | |
dc.contributor.author | Karadag, A | |
dc.contributor.author | Bulak, E | |
dc.contributor.author | Lonnecke, P | |
dc.date.accessioned | 2020-06-21T15:44:38Z | |
dc.date.available | 2020-06-21T15:44:38Z | |
dc.date.issued | 2003 | |
dc.identifier.issn | 0022-2860 | |
dc.identifier.uri | https://doi.org/10.1016/S0022-2860(02)00720-2 | |
dc.identifier.uri | https://hdl.handle.net/20.500.12712/21868 | |
dc.description | WOS: 000181383000015 | en_US |
dc.description.abstract | In the title complex, C22H36N4O10, cyclic eight-membered hydrogen bonded rings exist involving 2-aminopyridinium and adipate ions. Adipic acid molecules and adipate ions are linked in zigzag chains by O-H...O hydrogen bonds. The characteristic IR absorption bands of 2-aminopyridinium adipate monoadipic acid dihydrate were observed as; 35002500 cm(-1) region (hydrogen bonded O-H and N-H stretch), 1695 cm(-1) (carboxylic C=O stretch), 1595 cm(-1) (C=N ring stretching and N-H bending vibrations), 1565 and 1395 cm(-1) (asymmetrical and symmetrical stretch of carboxylate ion, respectively). The title complex showed two thermal decomposition steps. Crystallization water release in the first step (105-118 degreesC) and remaining anhydrous complex decomposition completely in the second step (120-450 degreesC). (C) 2003 Elsevier Science B.V. All rights reserved. | en_US |
dc.language.iso | eng | en_US |
dc.publisher | Elsevier Science Bv | en_US |
dc.relation.isversionof | 10.1016/S0022-2860(02)00720-2 | en_US |
dc.rights | info:eu-repo/semantics/closedAccess | en_US |
dc.subject | 2-aminopyridinium adipate | en_US |
dc.subject | 2-aminopyridinine | en_US |
dc.subject | adipic acid | en_US |
dc.subject | hydrogen bonding | en_US |
dc.subject | X-ray crystal structure | en_US |
dc.subject | IR | en_US |
dc.subject | TG | en_US |
dc.subject | DSC | en_US |
dc.title | Crystal structure, spectral and thermal properties of 2-aminopyridinium adipate monoadipic acid dihydrate | en_US |
dc.type | article | en_US |
dc.contributor.department | OMÜ | en_US |
dc.identifier.volume | 648 | en_US |
dc.identifier.issue | 01.Feb | en_US |
dc.identifier.startpage | 133 | en_US |
dc.identifier.endpage | 138 | en_US |
dc.relation.journal | Journal of Molecular Structure | en_US |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |