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Synthesis, experimental and theoretical characterization of palladium(II) and platinum(II) saccharinate complexes with 2-(2-pyridyl)benzimidazole

Date

2011

Author

Guney, Emel
Kaya, Yunus
Yılmaz, Veysel T.
Gumus, Sedat

Metadata

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Abstract

New palladium(II) and platinum(II) complexes of saccharinate (sac) with 2-(2-pyridyl)benzimidazole (pybim) have been synthesized and characterized by elemental analysis and spectroscopic techniques. From the experimental studies, these complexes were formulated as [Pd(pybim)(sac)(2)] (1), and [Pt(pybim)(sac)(2)]center dot 4H(2)O (2). The ground-state geometries of both complexes were optimized using density functional theory (DFT) methods at the B3LYP level. A bidentate pybim ligand together with two N-coordinated sac ligands form the square-planar MN4 coordination geometry around the palladium(II) and platinum(II) ions. The calculated IR and UV-vis spectral data have been correlated to the experimental results. Thermal analysis data support the molecular structures of both complexes. (C) 2011 Elsevier B.V. All rights reserved.

Source

Spectrochimica Acta Part A-Molecular and Biomolecular Spectroscopy

Volume

79

Issue

5

URI

https://doi.org/10.1016/j.saa.2011.04.038
https://hdl.handle.net/20.500.12712/17055

Collections

  • PubMed İndeksli Yayınlar Koleksiyonu [6144]
  • Scopus İndeksli Yayınlar Koleksiyonu [14046]
  • WoS İndeksli Yayınlar Koleksiyonu [12971]



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