Yazar "Kutuk, Halil" için listeleme
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Characterization and Comparative Studies on Conventional and Microwave Synthesis of Some Disulfides
Karakullukcu, Nalan Turkoz; Yakan, Hasan; Ozturk, Seyhan; Kutuk, Halil (Taylor & Francis Ltd, 2013)Some disulfide derivatives have been prepared by microwave assisted synthesis methodology from thiophthalimides(sulfenimides) and thiols in a modified microwave oven under reflux at 600 Watt in ethanol. Elucidation of the ... -
Comparison of conventional and microwave-assisted synthesis of some new sulfenamides under free catalyst and ligand
Yakan, Hasan; Kutuk, Halil (Springer Wien, 2018)Sulfenamide and its derivatives (S-N bond) have been synthesized with classical method in the literature. However, microwave-assisted synthesis of a series of N-(substituted phenylthio), N-(benzylthio), N-(cyclothio), and ... -
Crystal and Molecular Structure of N-(Phenylthio)phthalimide(1)
Tanak, Hasan; Yakan, Hasan; Kutuk, Halil; Karakullukcu, Nalan Turkoz; Dege, Necmi (Pleiades Publishing Inc, 2018)The title compound N-(Phenylthio)phthalimide has been synthesized and characterized by FT-IR, NMR, and X-ray single-crystal determination. The compound crystallizes in the triclinic sp. gr. P & Unknown; with Z= 2. The title ... -
Crystal Structure and DFT Calculations of Two Derivatives of Phthalimide.
Yazici, Serap; Turkoz, Nalan; Kutuk, Halil; Senel, Ismet; Büyükgüngör, Orhan (Int Union Crystallography, 2009)… -
Crystal structure of 2,3-dimethoxy-N-(4-nitrophenyl)benzamide
Yaman, Mavise; Almarhoon, Zainab M.; Cakmak, Sukriye; Kutuk, Halil; Meral, Gungor; Dege, Necmi (Int Union Crystallography, 2018)In the title compound, C15H14N2O5, the benzene rings are nearly coplanar, making a dihedral angle of 4.89 (8)degrees. An intramolecular N-H center dot center dot center dot O hydrogen bond occurs between the imino and ... -
Crystal Structure of 3-Acetoxy-2-methyl-N-(4-nitrophenyl)benzamide
Kansiz, Sevgi; Cakmak, Sukriye; Dege, Necmi; Meral, Gungor; Kutuk, Halil (Japan Soc Analytical Chemistry, 2018)The structure of 3-acetoxy-2-methyl-N-(4-nitrophenyl)benzamide was determined by X-ray crystallography. The compound crystallized in a monoclinic system and it was characterized in the space group P2(1)/c with cell parameters ... -
Investigation of the acid-catalyzed hydrolysis and reaction mechanisms of N,N '-diarylsulfamides using various criteria
Bekdemir, Yunus; Erturk, Aliye Gediz; Kutuk, Halil (Wiley-Blackwell, 2014)The mechanism of acidaEurocatalyzed hydrolysis of a series of paEurosubstituted N,NaEuro(2)aEurodiarylsulfamides was investigated in aqueous mineral acid solutions. Rate profiles, reaction activation parameters, catalytic ... -
A Kinetic Study of Acid-Catalyzed Hydrolysis of Some Arylsulfonyl Phthalimides
Kutuk, Halil; Ozturk, Seyhan (Taylor & Francis Ltd, 2009)The acid-catalyzed hydrolysis of arylsulfonyl phthalimides was studied in aqueous solutions of sulfuric, perchloric, and hydrochloric acid at 35.0 0.1C. Analysis of the data by the excess acidity method and activation ... -
The Mechanisms of Acid-Catalyzed Hydrolysis of N-(4-Substituted Arylthio) Phthalimides
Kutuk, Halil; Yakan, Hasan (Taylor & Francis Ltd, 2011)The acid-catalyzed hydrolysis of N-(4-substitutedarylthio)phthalimides was studied in aqueous solutions of sulfuric, perchloric, and hydrochloric acids at 40.0 +/- 0.1 degrees C. Analysis of the data by the excess acidity ... -
Microwave-Assisted Synthesis of Disulfides
Kutuk, Halil; Turkoz, Nalan (Taylor & Francis Ltd, 2011)A new microwave-assisted synthesis methodology for the preparation of substituted disulfide derivatives is presented. 4-Substituted sulfenimides were reacted with 4-substituted thiols under neat (to right doughy consistency) ... -
N-(p-methoxyphenylsulfanyl)phthalimide
Yazici, Serap; Turkoz, Nalan; Kutuk, Halil; Senel, Ismet; Büyükgüngör, Orhan (Blackwell Publishing, 2007)In the molecule of the title compound, C15H11NO3S, the dihedral angle between the phthalimide ring system and the benzene ring is 74.07 (8)degrees. -
N-[(4-Methylphenyl)sulfanyl]phthalimide
Yazici, Serap; Turkoz, Nalan; Kutuk, Halil; Senel, Ismet; Büyükgüngör, Orhan (Int Union Crystallography, 2007)In the title compound, C15H11NO2S, the dihedral angle between the two planar ring systems is 74.49 (5)degrees. -
A novel 3-acetoxy-2-methyl-N-(4-methoxyphenyl)benzamide: Molecular structural describe, antioxidant activity with use X-ray diffractions and DFT calculations
Demir, Sibel; Cakmak, Sukriye; Dege, Necmi; Kutuk, Halil; Odabaşoğlu, Mustafa; Kepekci, R. Aysun (Elsevier, 2015)In this work, the structure of a novel 3-acetoxy-2-methyl-N-(4-methoxyphenyl) benzamide, was analyzed both experimentally and theoretically using three methods, X-ray single crystal diffraction technique, IR spectroscopy, ... -
Phthalocyanines with bromobenzenesulfanyl substituents at non-peripheral position: Preparation, photophysical and photochemical properties
Atmaca, Goknur Yasa; Yakan, Hasan; Kutuk, Halil; Nebioglu, Mehmet; Guzel, Emre; Erdogmus, Ali (World Sci Publ Co Inc, 2019)Electron-donating bromobenzenesulfanyl-group-substituted phthalonitrile derivative (1) and its novel non-peripherally tetra-substituted metal-free, indium and zinc phthalocyanine complexes (2-4) have been prepared for the ... -
Spectroscopic Properties and Preparation of Some 2,3-Dimethoxybenzamide Derivatives
Cakmak, Sukriye; Kutuk, Halil; Odabaşoğlu, Mustafa; Yakan, Hasan; Büyükgüngör, Orhan (Bentham Science Publ Ltd, 2016)In this study, a series of substituted secondary amide compounds were synthesized starting from 2,3-dimethoxybenzoic acid and aniline derivatives. The structures of these synthesized compounds were determined using IR, H-1 ... -
The Synthesis and Acid-Catalyzed Hydrolysis of N-(4-Substitutedphenyl)-O-Benzenedisulfonimides
Bekdemir, Yunus; Eren, Bilge; Kutuk, Halil (Taylor & Francis Ltd, 2012)The acid catalyzed hydrolyses of some cyclic disulfonimides, N-(4-substitutedphenyl)-o-benzenedisulfonimides (1a-d) have been studied in concentrated aqueous acidic solutions. Analysis of the data by the Excess Acidity ... -
Synthesis and characterization of 3-acetoxy-2-methyl-N-(phenyl) benzamide and 3-acetoxy-2-methyl-N-(4-methylphenyl)benzamide
Kirca, Basak Kosar; Cakmak, Sukriye; Kutuk, Halil; Odabaşoğlu, Mustafa; Büyükgüngör, Orhan (Elsevier, 2018)This study treats about two successfully synthesized secondary amide compounds 3-Acetoxy-2-methyl-N-(phenyl)benzamide, I and 3-Acetoxy-2-methyl-N-(4-methylphenyl)benzamide, II. Compounds were characterized by FTIR, H-1 ... -
The Synthesis of Sulfinylphthalimides and Their Reactions With Some Nucleophiles in Dioxane
Bozkurt, Yasemin Soydas; Kutuk, Halil (Taylor & Francis Ltd, 2011)In this study, some N-(p-substituted-arylsulfinyl)phthalimides (1a-1e) were synthesized. The synthesized compounds were examined with respect to their substitution reactions with sodium ethoxide, sodium methoxide, methylamine, ... -
Synthesis, characterization, antioxidant, and antibacterial activities of new 2,3-dimethoxy and 3-acetoxy-2-methyl benzamides
Yakan, Hasan; Cakmak, Sukriye; Kutuk, Halil; Yenigun, Semiha; Ozen, Tevfik (Springer, 2020)We performed a series of novel benzamide compounds which were synthesized starting from 2,3-dimethoxybenzoic acid or 3-acetoxy-2-methylbenzoic acid and amine derivatives. All the obtained products were purified, and the ... -
Synthesis, crystal structure, spectroscopic features and Hirshfeld surfaces of 2-methyl-3-[(2-methylphenyl)carbamoyl]phenyl acetate
Yaman, Mavise; Cakmak, Sukriye; Dege, Necmi; Odabaşoğlu, Mustafa; Pavlenko, Vadim A.; Kutuk, Halil (Int Union Crystallography, 2019)The title compound, C17H17NO3, was synthesized, characterized by IR spectroscopy and its crystal structure was determined from single-crystal diffraction data. The asymmetric unit contains two molecules, which adopt different ...
