Yazar "Kazak, Canan" için listeleme
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Hydrothermal and sonochemical synthesis of a nano-sized 2D lead(II) coordination polymer: A precursor for nano-structured PbO and PbBr2
Aslani, Alireza; Morsali, Ali; Yılmaz, Veysel T.; Kazak, Canan (Elsevier, 2009)A new nano-structured lead(II) coordination polymer, [Pb(mu-bpp)(mu-Br)(2)](n) (PBB) [bpp = 1,3-di(4-pyridyl)propane], has been synthesized by the reaction of a mixture lead(II) acetate and KBr with bpp by both hydrothermal ... -
Influence of the crystallization solvent on the molecular structures of copper(II) saccharinato complexes with pyridazine: Synthesis, X-ray crystallography, spectroscopy, photoluminescence, and thermal properties
Yılmaz, Veysel T.; Senel, Evrim; Kazak, Canan (Csiro Publishing, 2008)X-Ray structural analysis has shown that the products of the reaction of [Cu(sac)(2)(H2O)(4)]center dot 2H(2)O (sac= saccharinate) with pyridazine (pydz) are markedly dependent on the solvent used in the crystallization. ... -
Iron(III) complex of a tridentate NNN type ligand: synthesis, X-ray structure, thermal analysis and voltammetric studies
Hopa, Cigdem; Alkan, Mahir; Kazak, Canan; Arslan, N. Burcu; Kurtaran, Raif (Springer, 2009)A mononuclear iron(III) complex with 2,6-bis(3,4,5-trimethyl-N-pyrazolyl)pyridine (btmpp) has been synthesized, and characterized by X-ray crystallography, IR, UV-Vis and TGA-DTA methods. The Fe(III/II) couple was characterized ... -
A luminescent silver-saccharinato complex with S,S-diphenylsulfimide: Synthesis, spectroscopic, thermal, structural and DFT computational studies
Gumus, Sedat; Hamamci, Sevim; Yilmaz, V. T.; Kazak, Canan (Elsevier, 2007)A new silver(l)-saccharinato (sac) complex with S,S-diphenylsulfimide, [Ag(sac)(Ph2SNH)], has been prepared and characterized by elemental analysis, IR spectroscopy, thermal analysis and single crystal X-ray diffraction. ... -
(+/-)-methyl 1-oxo-1H-spiro[benzo[c]pyran-3(4H), 1 '-cyclohexane]-4-carboxylate
Yildirim, Sema Ozturk; Akkurt, Mehmet; Bogdanov, Milen G.; Kandinska, Meglena I.; Kazak, Canan (Int Union Crystallography, 2007)The molecule of the title compound, C16H18O4, is non-planar and the pyran ring adopts a half-chair conformation. Intermolecular C-H (. . .) O hydrogen-bond contacts link the molecules in the crystal structure, forming ... -
Methyl 1H-1,2,3-triazole-4-carboxylate
Prabakaran, K.; Maiyalagan, T.; Hathwar, Venkatesha R.; Kazak, Canan; Khan, F. Nawaz (Int Union Crystallography, 2009)The title compound, C4H5N3O2, features an essentially planar molecule (r.m.s. deviation for all non-H atoms = 0.013 angstrom). The crystal structure is stabilized by intermolecular N-H center dot center dot center dot O ... -
N-(4-Nitrobenzoyl)-N '-(1,5-dimethyl-3-oxo-2-phenyl-1H-3(2H)-pyrazolyl)-thiourea hydrate: Synthesis, spectroscopic characterization, X-ray structure and DFT studies
Arslan, N. Burcu; Kazak, Canan; Aydin, Fatma (Pergamon-Elsevier Science Ltd, 2012)The title molecule (C19H17N5O4S center dot H2O) was synthesized and characterized by IR-NMR spectroscopy. MS and single-crystal X-ray diffraction. The molecular geometry, vibrational frequencies and gaugeindependent atomic ... -
A non-metallic ionic saccharinate. Synthesis, structure and DFT calculations of piperazinium disaccharinate
Gumus, Sedat; Guney, Serkan; Yılmaz, Veysel T.; Kazak, Canan (Wiley-V C H Verlag Gmbh, 2006)A new ionic saccharinate (sac) compound with the piperazinium dication (H(2)ppz)(sac)(2) (1), has been synthesized and characterized by elemental analysis, IR spectroscopy, and single crystal X-ray diffraction. The compound ... -
A novel 1D coordination polymer [Pb(phen)(mu-N-3)(mu-NO3)](n) with the first Pb-2-(mu-N-3)(2) unit (phen=1,10-phenanthroline)
Marandi, Farzin; Mirtamizdoust, Babak; Soudi, Ali A.; Yılmaz, Veysel T.; Kazak, Canan (Wiley-V C H Verlag Gmbh, 2006)A novel ID polymeric lead(II) complex containing the first Pb-2-(mu-N-3)(2) motif, [Pb(phen)(mu-N-3)(mu-NO3)](n) (phen = 1,10-phenanthroline), has been synthesized and characterized. The single-crystal X-ray data showed ... -
A novel two-dimensional silver(I) saccharinato coordination polymer constructed from weak Ag center dot center dot center dot C interactions: Synthesis, IR spectra and X-ray structure
Yılmaz, Veysel T.; Hamamci, Sevim; Kazak, Canan (Elsevier Science Sa, 2008)A new dinuclear silver(I)-saccharinato (sac) complex with acetonitrile (MeCN), [Ag-2(sac)(2)(MeCN)(2)](n) has been synthesized and characterized by elemental analysis, IR spectroscopy and single crystal X-ray diffraction. ... -
A one-dimensional pyrazine bridged Copper(II)-Saccharinato coordination polymer
Senel, Evrim; Yılmaz, Veysel T.; Kazak, Canan (Wiley-V C H Verlag Gmbh, 2008)A one-dimensional copper(II) complex {[Cu(sac)(2)(mu-pyz)(H2O)] center dot H2O}(n) (1) (pyz = pyrazine, and sac = saccharinate) has been synthesized and characterized by elemental analysis, IR spectroscopy, thermal and ... -
One-dimensional pyrazine bridged M(II)-saccharinato coordination polymers: Synthesis, characterization, crystal structures and thermal studies
Yılmaz, Veysel T.; Senel, Evrim; Kazak, Canan (Pergamon-Elsevier Science Ltd, 2007)Three new coordination polymers with a general formula [M(sac)(2)(mu-pyz)(H2O)(2)][M = Mn(II) (1), Fe(II) (2), Co(II) (3), pyz = pyrazine. and sac = saccharinate] have been synthesized and characterized by elemental analyses, ... -
Oxidovanadium(V) complexes containing hydrazone based O,N,O-donor ligands: Synthesis, structure, catalytic properties and theoretical calculations
Hosseini-Monfared, Hassan; Bikas, Rahman; Mahboubi-Anarjan, Parisa; Blake, Alexander J.; Lippolis, Vito; Arslan, N. Burcu; Kazak, Canan (Pergamon-Elsevier Science Ltd, 2014)Two new mono oxidovanadium(V) complexes, [VOL1(OEt)] (1) and [VOL2(OMe)] (2), of the tridentate Schiff base hydrazone-type O,N,O-donor ligands H2L1 and H2L2, obtained by monocondensation of 3-hydroxy-2-naphthohydrazide ... -
Spectroscopic and Quantum Chemical Studies of (Z)-N '-(3-(hidroksiimino)butan-2-ylidene)-4-metilbenzensulfonohidrazide Ligand
Guntepe, Feyizan; Cinarli, Murat; Kazak, Canan; Bati, Humeyra (Taylor & Francis Ltd, 2015)The structural and spectroscopic characterization of Schiff base ligand, (Z)-N'-(3-(hidroksiimino)butan-2-ylidene)-4metilbenzensulfonohidrazide (HL) are presented in this paper. The optimized geometry and vibrational ... -
Spectroscopic and structural study of Ni (II) dipicolinate complex with 2-amino-4-methylpyrimidine
Bulut, İclal; Uçar, İbrahim; Kazak, Canan (2009)Nickel(II) dipicolinate complex containing 2-amino-4-methylpyrimidine (2A-4Mpy), [Ni(2A-4Mpy)(dpc) {(H_2O)}_2] · 2H_2O was synthesized in solid state and its structural and spectroscopic properties were determined ... -
Spectroscopic and Structural Study of Ni(II) Dipicolinate Complex with 2-Amino-4-methylpyrimidine
Bulut, Iclal; Ucar, Ibrahim; Kazak, Canan (Scientific Technical Research Council Turkey-Tubitak, 2009)Nickel(II) dipicolinate complex containing 2-amino-4-methylpyrimidine (2A-4Mpy), [Ni(2A-4Mpy)(dpc) (H2O)(2)] center dot 2H(2)O was synthesized in solid state and its structural and spectroscopic properties were determined ... -
Structural characterization and EPR spectral studies on mononuclear copper(II) complex of saccharin with ethylnicotinate
Ucar, Ibrahim; Bozkurt, Esat; Kazak, Canan; Bulut, Ahmet (Pergamon-Elsevier Science Ltd, 2009)Mononuclear copper(II) saccharinate (sac) complex containing ethylnicotinate (enc). [Cu(enc)(2)(sac)(2) (H(2)O)]center dot 1.4H(2)O has been synthesized and characterized by spectroscopic (IR, UV-vis, EPR), X-ray diffraction ... -
Supramolecular lead(II) azide complex of 2,6-diacetylpyridine dihydrazone: synthesis, molecular structure, and biological activity
Kazak, Canan; Arslan, N. Burcu; Karabulut, Sedat; Azaz, A. Dilek; Namli, Hilmi; Kurtaran, Raif (Taylor & Francis Ltd, 2009)The complex of 2,6-diacetylpyridinedihydrazone (L) with lead(II) and azide has been characterized by elemental analyses, FTIR, and single-crystal X-ray analysis. The Pb(C9H13N11) (1) crystallized in the monoclinic space ... -
Synthesis and antidiabetic activity of 2,4-thiazolidindione, imidazolidinedione and 2-thioxo-imidazolidine-4-one derivatives bearing 6-methyl chromonyl pharmacophore
Unlusoy, Meltem Ceylan; Kazak, Canan; Bayro, Ornela; Verspohl, Eugen J.; Ertan, Rahmiye; Dundar, Oya Bozdag (Taylor & Francis Ltd, 2013)Numerous compounds have been prepared in order to improve the pharmacological profile of insulinotropic activities. In the present paper, we report the synthesis and the in vitro insulin releasing activity of the ... -
Synthesis and characterisations of some new 2,4-dihydro-[1,2,4]-triazol-3-one derivatives and X-ray crystal structures of 4-(3-phenylallylideneamino)-5-thiophen-2-yl-methyl-2,4-dihydro-[1,2,4]triazol-3-one
Sancak, Kemal; Unver, Yasemin; Kazak, Canan; Dugdu, Esra; Arslan, Burcu (Scientific Technical Research Council Turkey-Tubitak, 2010)Compounds 2 were synthesised via the reaction of 4-amino-5-thiophen-2-yl-methyl-2,4-dihydro-[1,2,4]triazol- 3-one (1) with aldehydes. Compounds 3 and 4 were obtained from compounds 2 with bromo acetophenone and ethyl ...