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Holodirected Coordination Sphere Around Lead(II) in Three-Dimensional Polymeric Structure; New Precursor for Preparation of Lead Oxide Sulfate Nano-Structures

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dc.authorscopusid15764796900
dc.authorscopusid20733771400
dc.authorscopusid58038557300
dc.authorscopusid58717985000
dc.authorscopusid36039473500
dc.contributor.authorAkhbari, K.
dc.contributor.authorBeheshti, S.
dc.contributor.authorMorsali, A.
dc.contributor.authorYilmaz, V.T.
dc.contributor.authorBüyuk̈güngör, O.
dc.date.accessioned2020-06-21T13:53:05Z
dc.date.available2020-06-21T13:53:05Z
dc.date.issued2014
dc.departmentOndokuz Mayıs Üniversitesien_US
dc.department-temp[Akhbari] Kamran, School of Chemistry, University of Tehran, Tehran, Tehran, Iran; [Beheshti] Saeideh, Department of Chemistry, Tarbiat Modares University, Tehran, Tehran, Iran; [Morsali] Ali, Department of Chemistry, Tarbiat Modares University, Tehran, Tehran, Iran; [Yilmaz] Veysel T., Department of Chemistry, Bursa Uludağ Üniversitesi, Bursa, Bursa, Turkey; [Büyuk̈güngör] Orhan, Department of Physics, Ondokuz Mayis Üniversitesi, Samsun, Turkeyen_US
dc.description.abstractA new lead(II) three-dimensional coordination polymer, [Pb <inf>2</inf>(μ<inf>3</inf>-ANS)<inf>2</inf>(μ<inf>2</inf>-Cl) <inf>2</inf>(H<inf>2</inf>O)<inf>2</inf>]<inf>n</inf> (1) [ANS- = 4-amino-1-naphthalenesulfonate], has been synthesized and characterized. The single-crystal X-ray data of compound 1 shows only one type of PbII ion with coordination number of six, the lead atom has distorted octahedral coordination sphere containing stereo-chemically inactive electron lone pair. The thermal stability of 1 was studied by TG-DTA (Thermo gravimetric and differential thermal analyses). Regular morphology of Pb<inf>2</inf>(SO <inf>4</inf>)O nano-particle was prepared from fine powders of compound 1 by calcination process at 700 °C. This nano-structure was characterized by XRD (X-ray powder diffraction) and SEM (Scanning electron microscopy). © 2014 Elsevier B.V. All rights reserved.en_US
dc.identifier.doi10.1016/j.molstruc.2014.06.004
dc.identifier.endpage283en_US
dc.identifier.issn0022-2860
dc.identifier.scopus2-s2.0-84903744929
dc.identifier.scopusqualityQ1
dc.identifier.startpage279en_US
dc.identifier.urihttps://doi.org/10.1016/j.molstruc.2014.06.004
dc.identifier.volume1074en_US
dc.identifier.wosWOS:000340315200035
dc.identifier.wosqualityQ2
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofJournal of Molecular Structureen_US
dc.relation.journalJournal of Molecular Structureen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCoordination Polymeren_US
dc.subjectHolodirecteden_US
dc.subjectLead Oxide Sulfateen_US
dc.subjectLead(II)en_US
dc.subjectNano-Particleen_US
dc.titleHolodirected Coordination Sphere Around Lead(II) in Three-Dimensional Polymeric Structure; New Precursor for Preparation of Lead Oxide Sulfate Nano-Structuresen_US
dc.typeArticleen_US
dspace.entity.typePublication

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