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Synthesis, spectroscopic (FT-IR/NMR) characterization, X-ray structure and DFT studies on (E)-2-(1-phenylethylidene) hydrazinecarboximidamide nitrate hemimethanol
(Pergamon-Elsevier Science Ltd, 2013)
The title molecular salt, (E)-2-(1-phenylethylidene) hydrazinecarboximidamide nitrate hemimethanol (C9H13N4+center dot NO3-center dot 0.5CH(4)O), was synthesized and characterized by elemental analysis, FT-IR and NMT ...
Synthesis and characterization of SiO2-supported ruthenium complexes containing aromatic sulfonamides: as catalysts for transfer hydrogenation of acetophenone
(Royal Soc Chemistry, 2013)
3-Amino-N-aryl-benzenesulfonamides (1-3) were successfully synthesized by the reaction of m-phenylenediamine and various benzenesulfonyl chlorides. Then, a series of ruthenium complexes (4-6) were prepared from the reaction ...
Synthesis and catalytic activity of ruthenium(II) complexes containing pyridine-based tridentate triamines ('NNN') and pyridine carboxylate ligands (NO)
(Elsevier Science Sa, 2012)
The reaction of [(p-cymene)RuCl2](2) with K[NOa-b] (NO- = 2-picolinate, a or 2-quinaldinate, b) gave neutral [(p-cymene)RuCl(NOa-b)] (1a-b), complexes which were treated with pyridine-based meridional triamine ligands ...
Synthesis, X-ray crystal structures, thermal and electrochemical properties of thiosemicarbazidatodioxouranium(VI) complexes
(Royal Soc Chemistry, 2010)
The stable uranyl complexes, [UO2(L)C9H19OH], were obtained from 3,5-dichlorosalicyl-(L-I) and salicyl-aldehyde-S-propyl-thiosemicarbazones (L-II) with substituted-salicylaldehyde in nonyl alcohol. The structures of the ...
Methyl 2-methoxy-7-(4-methylbenzoyl)-4-oxo-6-p-tolyl-4H-furo[3,2-c]pyran-3-carboxylate: A combined experimental and theoretical investigation
(Springer, 2009)
The title compound, methyl 2-methoxy-7-(4-methylbenzoyl)-4-oxo-6-p-tolyl-4H-furo[3,2-c]pyran-3-carboxylate (C25H20O7), was prepared and characterized by IR and single-crystal X-ray diffraction (XRD). The compound crystallizes ...
A mu-chloro-bridged dinuclear ruthenium complex with 9H-carbazole: the formation of one-dimensional linear chains of star-shaped edge-fused rings
(Blackwell Publishing, 2006)
The title complex, di-mu-chloro-bis[chloro(eta(6)-p-cymene)ruthenium(II)]-9H-carbazole (1/2), [Ru2Cl4(C10H14)(2)](.)2C(12)H(9)N, is composed of one [RuCl2(eta(6)-p-cymene)](2) and two 9H-carbazole molecules. There are ...
N-cyclohexyl-2-[5-(4-pyridyl)-4-(p-tolyl)-4H-1,2,4-triazol-3-ylsulfanyl]-acetamide dihydrate
(Int Union Crystallography, 2006)
In the title compound, C22H25N5OS center dot 2H(2)O, the molecules are stacked in columns running along the b axis. In this arrangemant, the molecules are linked to each other by a combination of one two-centre N-(HO)-O-... ...
Brorno(eta(4)-cycloocta-1,5-diene)[1-(2,3,4,5,6-pentafluorobenzyl)-3-(2, 4,6-trimethylbenzyl benzimidazol-2-ylidenel rhodium(I)
(Int Union Crystallography, 2006)
The title complex, [RhBr(C8H12)(C24H19F5N2)], has a distorted pseudo-square- planar geometry. The Rh-C bond distance between the N-heterocyclic ligand and the metal atom is 2.022 (3) angstrom. The angle between the carbene ...
